4. Hull synthesis
The rigid silica shell is synthesized in situ using a sol-gel process . Simple chemical reactions (hydrolysis and condensation) carried out at room temperature result in an inorganic polymer. The synthesis is carried out by the addition of a monomer, or silica precursor: tetraethylorthosilicate Si(OC2H5)4 denoted TEOS. TEOS is first hydrolyzed with the formation of silicic acid Si(OH)4 and alcohol (ROH). In a second step, a condensation reaction [polymerization through...
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Hull synthesis