1. Preparation
The polycondensation reaction is a balanced reaction between the end groups —NH2 (amine) and —COOH (acid) leading to the formation of —CONH— (amide) groups and water.
The polymer obtained at the end of the reaction, possibly in the presence of a chain limiter, therefore still contains a certain amount of water, residual monomer(s) and oligomers.
Careful drying is necessary before subsequent use, otherwise there is a risk of equilibrium displacement with a reduction in molecular weight.
Melt polyaddition/polycondensation and low-temperature solution polycondensation are still the most commonly used industrial methods.
Processes can be batch or continuous, single or multi-stage, with in some cases a melt or solid state...
You do not have access to this resource.
Exclusive to subscribers. 97% yet to be discovered!
Already subscribed?
Log in!
Ongoing reading
Preparation