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Differential scanning calorimetry with modulated temperature (TMDSC)

Article REF: P1206 V1

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Differential scanning calorimetry with modulated temperature (TMDSC)

Authors : Jean GRENET, Bernard LEGENDRE

Publication date: March 10, 2011, Review date: September 13, 2019 | Lire en français

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2. Information

All the experimental information is contained, on the one hand, in the measurement of the temperature modulated with time and therefore of the velocity β (t ) and, on the other hand, in that of the heat flux modulated (sample response) with time.

2.1 DSC-TM signals

Unlike conventional DSC, in DSC-TM the furnace temperature is programmed according to the law :

θ = θ_{0} + β_{0} t + A sin ω t

^( 7 )

...

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Bibliography

(1) - SCHAWE (J.E.K.), HÜTTER (T.), HEITZ (C.), ALIG (I.), LELLINGER (D.) - Stochastic temperature modulation : a new technique in temperature-modulated DSC. - Thermochimica Acta., 446, p. 147-155 (2006).
(2) - SCHUBNELL (M.), HEITZ (C.), HÜTTER (T.), SCHAWE (J.E.K.) -...

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