4. How to Make the Most of Your Experience
4.1 Alignment
Angular accuracy is essential for interpreting a diffractogram. An adjustment can be made using a direct beam: ensure that when the source and detector are directly opposite each other, the angle is zero. One can also use a reference sample, such as a silicon powder pellet (§ 4.2 ), and calibrate the equipment so that the positions of the standard’s peaks correspond exactly to the expected theoretical positions
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How to Make the Most of Your Experience
Description of a diffractogram
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